DCT Turbo Desktop Carbon Coater for SEM/TEM Sample Prep

DESKTOP CARBON COATERS

SEM/TEM Preparation Carbon Coater, Low and high vacuum systems

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Description

Sample preparation using Carbon coating is the recognised method for non-conductive and low conductive specimens or samples.

The DCT system is a versatile carbon evaporator for preparing specimens for electron microscopy or EDXA analysis. It has been designed as a high-current power supply capable of evaporating both carbon rod and carbon fibre. In other words, it can coat carbon on different types of substrates for X-Ray analysis and coating conducting carbon fibre & rod for SEM analysis.
The excellent design of the system enables the user to easily load and unload samples, and quickly replace the carbon fibre/rod. The system is equipped with a film thickness monitor (FTM), which measures the coating thickness on a quartz crystal mounted in the vacuum chamber with an accuracy of 1 nm. The system can automatically terminate a coating cycle when the required thickness or time has been achieved..

The compact and easy to use carbon coater has the option of using existing pumps or supplied with a pump.

For external pumping, the onboard computer controls the pump or pumping rig.

Larger samples can be accommodated with our increased vacuum chamber DCR-L and DCT-L system

Carbon Coating
Due to its excellent transparency and good electrical conductivity, deposited carbon thin films are widely used for either electron microscopy (EM) or X-ray microanalysis applications such as:
• support films for TEM (high vacuum (HV) evaporation) Carbon Coater
• conductive films for SEM/EDS samples (low vacuum evaporation)
• conductive surface films for non-conductive microprobe samples (HV evaporation)
• conductive surface films for non-conductive EBSD samples (HV evaporation)
• conductive surface films for non-conductive FESEM samples (HV evaporation) Carbon Coater
• conductive surface films for non-conductive FIB samples (HV evaporation)

Our board computer integration makes the Desktop Sputter coater an ideal laboratory and research tool for scanning electron microscopy (SEM) and Tunnelling electron microscopy analysis(TEM).

Thin films of about 5 nm (50Å) are used for particle support and as an isolating layer in autoradiography. Thicker films are also used in SEM and X-Ray Microanalysis. In general, deposited thin films should be uniformed with fine grain sizes and reproducible film thickness.

Carbon rod and carbon fibre are the two widely used sources for carbon evaporation in laboratories around the world. They each have their own features that make them of specific interests to the users. For a better understanding, further details of these features are presented in the following sections.

Carbon Rod versus Carbon Fibre Evaporation – Carbon Coater

Evaporating carbon thread or a pre-shaped carbon rod are both common methods to evaporate carbon. Using pre-shaped rods with the correct control system (pulse, continuous and auto) delivers a high-quality carbon layer and also gives good control over the thickness of the carbon layer. However, some users prefer to use carbon fibre because it has a faster and simpler process comparing with a carbon rod.

Applications

  • DCT: scanning electron microscope (SEM),High resolution
  • DCT: Transmission electron microscope (TEM).High resolution
  • DCT:X-Ray analysis (EDX). High resolution
  • DCT:EDS/WDS and thin film applications.
  • DCT:FE-SEM.
  • DCT:ETEM .
  • DCT:EBSD

Features

  • DCR; rotary pumped coater.
  • quartz crystal thickness monitor.
  • Touch screen control.
  • Rapid data input.
  • User friendly software.
  • Accurate Control of coating rate.
  • record and plot coating parameters graphs.
  • Manual Control option for Time and Thickness.
  • Manual settings, Time, Thickness and power.
  • Automatic Timed and Thickness li>
  • Rotation stage as standard.
  • Pulsed Carbon Fibre Evaporation.
  • Two-year warranty
  • CE conformity

Vac Coat DCT Specifications

  • DCT: High vacuum turbo pump 70 l/s.
  • DCT: Diaphragm backing pump.
  • DCT: Full range vacuum gauge.
  • Pyrex cylinder chamber 0 mm OD x 140 mm.
  • DC power supply 0-100 A switching Pulsed.
  • DCT: Ultimate Vacuum: Less than 2 x 10-5 torr.
  • Dimensions: 450 x 500 x 370 mm (H x W x D).
  • Utilities: 220V-50Hz – 10A.
  • Coloured touch screen display.
  • Sample holder with rotation.
  • Electronic shutter.
  • Automatically controlled coating.Pressure independent
  • Precision metering valve for fine control of vacuum pressure.
  • USB port for export of datali>
  • Shipping Weight: 46 Kg.

Options and Accessories

  • The DCR and DCT have the flowing options and accessories:
  • Quartz crystal
  • Planetary Sample rotation
  • Spare glass
  • Carbon Fibre

Carbon Rod Evaporation

Features of carbon rod evaporation

  • High purity carbon rods with low surface area remain pure
  • Thickness can be controlled between 1-50nm from a single rod
  • Control over power and evaporation time determines thickness
  • Clean carbon layer
  • High power supply with pulse is required
  • Multiple evaporation is possible with one set of rods
  • Pulse mode without breaking vacuum can be used to build up a thick carbon layer

Carbon Fibre Flash evaporation

Features of carbon rod evaporation

  • High surface area of the carbon fibres has more adsorbed contaminants
  • Diameter of braided carbon thread determine thickness, not really variable
  • Flash evaporation without control
  • Carbon fibres tend to fall on surface causing imaging artifacts
  • lower size power supply, approx. 50A
  • Single evaporation process, source needs reloading after each evaporation
  • Thicker layers can be built up by using multiple threads or braids